Organic pollutants in water
For analyzing organic pollutants in water, the compounds may be pre-concentrated by extraction with an organic solvent. You have the job to determine the concentration of 1-naphthol in a contaminated groundwater by using gas chromatography.
You decide to extract 20 mL water samples with a convenient solvent:
ethylacetate at 25°C: Ki ethylacetate / water = 102.60 [L water /L ethylacetate ].
Now you wonder how much ethyl acetate you should use. Calculate the volume of ethylacetate that you need at minimum if you want to extract at least 99% of the total 1-naphthol from the water sample. Are you happy with this pre-concentration step? Somebody tells you that it would be much wiser to extract the sample twice with the goal to get each time 90% of the compound out of the water (which would also amount to an extraction efficiency of 99% in total), and then pool the two extracts.
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Proceed |
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