Sample preparation

Sample preparation - context
Sample preparation - motivation
Purpose of sample preparation
Overview of preparation methods
     Liquid liquid extraction (LLE)
     Solid phase extraction (SPE)
     Solid phase microextraction (SPME)
     Purge and trap (PT)
     (Accelerated) Solvent extraction ((A)SE)
     Supercritical fluid extraction (SFE)
      Filter Techniques (FT)
Box 10 Filtration
Box 11 Sorbents
Box 12 Preconcentration
Self test
Problems
End of chapter


Overview of preparation methods

Routine methods that are employed in environmental trace analysis.

Extraction phase
Sample matrix
containing analyte
into which analyte
is transferred

liquid

solid

gaseous

liquid

 

- Liquid-liquid extraction (LLE)  
- (Accelerated) Solvent extraction ((A)SE)
- Supercritical fluid extraction (SFE)

___
 

solid

 

- Solid phase extraction (SPE)
- Solid phase microextraction (SPME)

___
 
- Solid phase microextraction (SPME)
- Filter techniques (FT)

gaseous

 

- Purge and trap (PT)
- Supercritical fluid extraction (SFE)
___